Synthesis of 2-(4'-Diethylamino-1'-methylbutylamino)-4-phenylquinoline and a 6-Chloro Derivative

GA Reynolds, CR Hauser

Index: Reynolds; Hauser Journal of the American Chemical Society, 1950 , vol. 72, p. 1852

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Citation Number: 4

Abstract

Experimental Hydrogenation of the Stilbazole Methiodides.-The pure stilbazole methiodide (0.02-0.05 M) was dissolved or sus-pended in absolute methanol (50-100 cc.), approximately 0.2 g. of A dam catalyst was added, and the hydrogenation was carried out in a Burgess-Parr catalytic hydrogenation apparatus with shaking at two to three atmospheres overpressure of hydrogen. Hydrogen uptake proceeded rapidly (usually complete in one ...