The Journal of organic chemistry

Microwave-assisted one-pot synthesis of 1-indanones from arenes and α, β-unsaturated acyl chlorides

W Yin, Y Ma, J Xu, Y Zhao

Index: Camps, F.; Coll, J.; Colomina, O.; Messeguer, A. Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 12 p. 1801 - 1805

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Citation Number: 74

Abstract

... Between the two irradiations, the reaction temperature was allowed to cool to about 60 °C. After hydrolysis by addition of concentrated hydrochloric acid (15 mL) and ... Mp 68−70 °C. R f = 0.38 [ethyl acetate/ petroleum ether (60−90 °C) 1:15, v/v, silica gel plate ... 1) For examples, see ...