Improved procedures for the preparation of cycloalkyl-, arylalkyl-, and arylthioureas

…, FJ Villani Jr, LE Weaner, BE Reynolds, AR Hood…

Index: Rasmussen, C. R.; Villani, F. J.; Weaner, L. E.; Reynolds, B. E.; Hood, A. R.; et al. Synthesis, 1988 , # 6 p. 456 - 459

Full Text: HTML

Citation Number: 91

Abstract

© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular ...

 Related Synthetic Route
N-benzoyl-N'-(3,4-dichlorophenyl)thiourea Structure

19249-85-5

N-benzoyl-N'-(3...

~89%

1-(3,4-Dichlorophenyl)-2-thiourea Structure

19250-09-0

1-(3,4-Dichloro...

4-Aminophenol Structure

123-30-8

4-Aminophenol

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~96%

Benzamide, N-[[ (4-hydroxyphenyl)amino]thioxomethyl]- Structure

5461-34-7

Benzamide, N-[[...

N-(pyridin-3-ylcarbamothioyl)benzamide Structure

30162-36-8

N-(pyridin-3-yl...

~89%

3-pyridylthiourea Structure

30162-37-9

3-pyridylthiourea

Benzamide,N-[[(2,3-dichlorophenyl)amino]thioxomethyl]- Structure

83697-81-8

Benzamide,N-[[(...

~95%

1-(2,3,4,5,6-PENTAMETHYLPHENYL)-2-PHENYLETHAN-1-ONE Structure

41542-06-7

1-(2,3,4,5,6-PE...

Benzamide, N-(((4-(dimethylamino)phenyl)amino)thioxomethyl)- (9CI) Structure

6281-64-7

Benzamide, N-((...

~82%

1-[4-(dimethylamino)phenyl]-2-thiourea Structure

22283-43-8

1-[4-(dimethyla...

N/A Structure

31437-19-1

N/A

~57%

1-(PYRIMIDIN-2-YL)THIOUREA Structure

31437-20-4

1-(PYRIMIDIN-2-...

N-{[4-(2-Methyl-2-propanyl)phenyl]carbamothioyl}benzamide Structure

117174-73-9

N-{[4-(2-Methyl...

~96%

4-TERT-BUTYL-PHENYLTHIOUREA Structure

65259-90-7

4-TERT-BUTYL-PH...

3,5-Dimethylaniline Structure

108-69-0

3,5-Dimethylaniline

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~87%

N-[(3,5-Dimethylphenyl)carbamothioyl]benzamide Structure

117174-79-5

N-[(3,5-Dimethy...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(3,5-Dimethylphenyl)carbamothioyl]benzamide Structure

117174-79-5

N-[(3,5-Dimethy...

N-[(3,5-Dimethylphenyl)carbamothioyl]benzamide Structure

117174-79-5

N-[(3,5-Dimethy...

~87%

3,5-dimethylphenylthiourea Structure

97480-60-9

3,5-dimethylphe...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

3,4-Dimethoxyaniline Structure

6315-89-5

3,4-Dimethoxyaniline

~92%

Benzamide,N-[[(3,4-dimethoxyphenyl)amino]thioxomethyl]- Structure

65069-48-9

Benzamide,N-[[(...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

Benzamide,N-[[(3,4-dimethoxyphenyl)amino]thioxomethyl]- Structure

65069-48-9

Benzamide,N-[[(...

2-Ethylaniline Structure

578-54-1

2-Ethylaniline

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~95%

N-[(2-ethylphenyl)carbamothioyl]benzamide Structure

88884-36-0

N-[(2-ethylphen...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(2-ethylphenyl)carbamothioyl]benzamide Structure

88884-36-0

N-[(2-ethylphen...

2-(Prop-1-en-2-yl)aniline Structure

52562-19-3

2-(Prop-1-en-2-...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~96%

N-[(2-prop-1-en-2-ylphenyl)carbamothioyl]benzamide Structure

88884-37-1

N-[(2-prop-1-en...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(2-prop-1-en-2-ylphenyl)carbamothioyl]benzamide Structure

88884-37-1

N-[(2-prop-1-en...

N-((3-chloro-2-methylphenyl)carbamothioyl)benzamide Structure

117174-75-1

N-((3-chloro-2-...

~94%

1-(3-Chloro-2-methylphenyl)-2-thiourea Structure

63980-70-1

1-(3-Chloro-2-m...

3-benzoyl-1-(4-chloro-2-methylphenyl)-2-thiourea Structure

71233-05-1

3-benzoyl-1-(4-...

~99%

1-(4-BROMOPHENYLSULFONYL)PIPERIDINE Structure

63980-71-2

1-(4-BROMOPHENY...

N-[(2-chloro-4-methyl-phenyl)thiocarbamoyl]benzamide Structure

71233-09-5

N-[(2-chloro-4-...

~98%

(2-chloro-4-methyl-phenyl)thiourea Structure

57005-14-8

(2-chloro-4-met...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

Benzamide,N-[[(2,3-dichlorophenyl)amino]thioxomethyl]- Structure

83697-81-8

Benzamide,N-[[(...

Benzamide,N-[[(3,4-dimethoxyphenyl)amino]thioxomethyl]- Structure

65069-48-9

Benzamide,N-[[(...

~97%

Thiourea,N-(3,4-dimethoxyphenyl)- Structure

65069-52-5

Thiourea,N-(3,4...

4-Aminobenzotrifluoride Structure

455-14-1

4-Aminobenzotri...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~92%

N-{[4-(Trifluoromethyl)phenyl]carbamothioyl}benzamide Structure

117174-71-7

N-{[4-(Trifluor...

3-(Trifluoromethyl)aniline Structure

98-16-8

3-(Trifluoromet...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~91%

N-Benzoyl-N'-[3-(trifluoromethyl)phenyl]thiourea Structure

89069-94-3

N-Benzoyl-N'-[3...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-Benzoyl-N'-[3-(trifluoromethyl)phenyl]thiourea Structure

89069-94-3

N-Benzoyl-N'-[3...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

2,6-Dichloroaniline Structure

608-31-1

2,6-Dichloroaniline

~96%

N-[(2,6-dichlorophenyl)carbamothioyl]benzamide Structure

41542-10-3

N-[(2,6-dichlor...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(2,6-dichlorophenyl)carbamothioyl]benzamide Structure

41542-10-3

N-[(2,6-dichlor...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

2-Chloro-4-methylaniline Structure

615-65-6

2-Chloro-4-meth...

~92%

N-[(2-chloro-4-methyl-phenyl)thiocarbamoyl]benzamide Structure

71233-09-5

N-[(2-chloro-4-...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(2-chloro-4-methyl-phenyl)thiocarbamoyl]benzamide Structure

71233-09-5

N-[(2-chloro-4-...

N,N-Dimethyl-1,4-benzenediamine Structure

99-98-9

N,N-Dimethyl-1,...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~85%

Benzamide, N-(((4-(dimethylamino)phenyl)amino)thioxomethyl)- (9CI) Structure

6281-64-7

Benzamide, N-((...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

Benzamide, N-(((4-(dimethylamino)phenyl)amino)thioxomethyl)- (9CI) Structure

6281-64-7

Benzamide, N-((...

N-[(4-propan-2-ylphenyl)thiocarbamoyl]benzamide Structure

80967-50-6

N-[(4-propan-2-...

~92%

1-(4-Isopropylphenyl)-2-thiourea Structure

65259-91-8

1-(4-Isopropylp...

N-((3-chloro-4-methylphenyl)carbamothioyl)benzamide Structure

117174-76-2

N-((3-chloro-4-...

~97%

1-(3-CHLORO-3-PHENYLPROPYL)PYRROLIDINEHYDROCHLORIDE Structure

117174-84-2

1-(3-CHLORO-3-P...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

4-Fluoroaniline Structure

371-40-4

4-Fluoroaniline

~86%

Benzamide,N-[[(4-fluorophenyl)amino]thioxomethyl]- Structure

399-07-5

Benzamide,N-[[(...

4-Isopropylaniline Structure

99-88-7

4-Isopropylaniline

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~67%

N-[(4-propan-2-ylphenyl)thiocarbamoyl]benzamide Structure

80967-50-6

N-[(4-propan-2-...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(4-propan-2-ylphenyl)thiocarbamoyl]benzamide Structure

80967-50-6

N-[(4-propan-2-...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

5-Chloro-2-methylaniline Structure

95-79-4

5-Chloro-2-meth...

~94%

N-[(5-chloro-2-methylphenyl)carbamothioyl]benzamide Structure

82635-63-0

N-[(5-chloro-2-...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(5-chloro-2-methylphenyl)carbamothioyl]benzamide Structure

82635-63-0

N-[(5-chloro-2-...

N-[(2-prop-1-en-2-ylphenyl)carbamothioyl]benzamide Structure

88884-37-1

N-[(2-prop-1-en...

~86%

(2-prop-1-en-2-ylphenyl)thiourea Structure

88884-39-3

(2-prop-1-en-2-...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-(pyridin-3-ylcarbamothioyl)benzamide Structure

30162-36-8

N-(pyridin-3-yl...

4-Chloroaniline Structure

106-47-8

4-Chloroaniline

~%

4-CHLOROPHENYLTHIOUREA Structure

3696-23-9

4-CHLOROPHENYLT...

Benzamide, N-[[ (4-hydroxyphenyl)amino]thioxomethyl]- Structure

5461-34-7

Benzamide, N-[[...

~99%

1-(4-HYDROXYPHENYL)-2-THIOUREA Structure

1520-27-0

1-(4-HYDROXYPHE...

N-{[4-(Trifluoromethyl)phenyl]carbamothioyl}benzamide Structure

117174-71-7

N-{[4-(Trifluor...

~88%

4-(Trifluoromethyl)phenylthiourea Structure

1736-72-7

4-(Trifluoromet...

N-((4-ethylphenyl)carbamothioyl)benzamide Structure

117174-72-8

N-((4-ethylphen...

~86%

1-(4-ETHOXYPHENYL)-2-THIOUREA Structure

22265-78-7

1-(4-ETHOXYPHEN...

3-anisidine Structure

536-90-3

3-anisidine

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~93%

Benzamide,N-[[(3-methoxyphenyl)amino]thioxomethyl]- Structure

21258-09-3

Benzamide,N-[[(...

3-Chloroaniline Structure

108-42-9

3-Chloroaniline

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

~86%

Urea, 1-benzoyl-3-(3-chlorophenyl)-2-thio- Structure

21258-04-8

Urea, 1-benzoyl...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

5-Chloro-2-methoxyaniline Structure

95-03-4

5-Chloro-2-meth...

~82%

N-[(5-chloro-2-methoxyphenyl)carbamothioyl]benzamide Structure

67618-11-5

N-[(5-chloro-2-...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(5-chloro-2-methoxyphenyl)carbamothioyl]benzamide Structure

67618-11-5

N-[(5-chloro-2-...

N-[(2-ethylphenyl)carbamothioyl]benzamide Structure

88884-36-0

N-[(2-ethylphen...

~92%

1-(2-ETHOXYPHENYL)-1H-PYRROLE-2,5-DIONE Structure

22265-77-6

1-(2-ETHOXYPHEN...

N-[(5-chloro-2-methoxyphenyl)carbamothioyl]benzamide Structure

67618-11-5

N-[(5-chloro-2-...

~81%

Thiourea,N-(5-chloro-2-methoxyphenyl)- Structure

63980-69-8

Thiourea,N-(5-c...

N-[(5-chloro-2-methylphenyl)carbamothioyl]benzamide Structure

82635-63-0

N-[(5-chloro-2-...

~94%

1-(5-CHLORO-2-METHYLPHENYL)-2-THIOUREA Structure

72806-61-2

1-(5-CHLORO-2-M...

N-Benzoyl-N'-[3-(trifluoromethyl)phenyl]thiourea Structure

89069-94-3

N-Benzoyl-N'-[3...

~86%

Thiourea,N-[3-(trifluoromethyl)phenyl]- Structure

1736-70-5

Thiourea,N-[3-(...

Urea, 1-benzoyl-3-(3-chlorophenyl)-2-thio- Structure

21258-04-8

Urea, 1-benzoyl...

~90%

1-(3-CHLOROPHENYL)-2-THIOUREA Structure

4947-89-1

1-(3-CHLOROPHEN...

N-((2-isopropylphenyl)carbamothioyl)benzamide Structure

25343-23-1

N-((2-isopropyl...

~98%

1-(2-ISOPROPYLPHENYL)-2-THIOUREA Structure

25343-32-2

1-(2-ISOPROPYLP...

benzoylthiocarbimide Structure

532-55-8

benzoylthiocarbimide

2-Bromoaniline Structure

615-36-1

2-Bromoaniline

~93%

N-[(2-Bromophenyl)carbamothioyl]benzamide Structure

5391-29-7

N-[(2-Bromophen...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(2-Bromophenyl)carbamothioyl]benzamide Structure

5391-29-7

N-[(2-Bromophen...

N-benzoyl-N'-(2-pyridyl)thiourea Structure

4921-86-2

N-benzoyl-N'-(2...

~86%

1-Pyridin-2-ylthiourea Structure

14294-11-2

1-Pyridin-2-ylt...

Usaf k-1471 Structure

4949-88-6

Usaf k-1471

~96%

1-(2-Methylphenyl)thiourea Structure

614-78-8

1-(2-Methylphen...


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