A mechanistic study of the C–P bond cleavage reaction of 1, 2-(PH 2) 2-C 6 H 4 with n BuLi/Sb (NMe 2) 3

R Edge, RJ Less, V Naseri, EJL McInnes…

Index: Dalton Transactions, , # 45 p. 6454 - 6460

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Citation Number: 4

Abstract

... DOI: 10.1039/B810028D (Paper) Dalton Trans., 2008 ... The resulting orange suspension was stirred (45 min) and then the solid dissolved by the addition of THF (1.0 mL) and heating ... 31 P{ 1 H} NMR (161.97 MHz, 25 °C, d 8 -THF); δ/ppm = −123.7 [|J XX ′| = 262.3, |J AX | = 172.0 ...