... 200 mL of methylene chloride. The lower, organic layer was dried over MgSO,, filtered, and solvent distilled through a 10-in. Vigreux column. ... (2) (a) Shultes, RE; Hofmann, A. "The Botany and Chemistry of Hallucinogens ... 2 I Y?.?. J. Org. Chem., Vol. 49, No. 24, 1984 4717 (B) ...