e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
Determination of peptide backbone torsion angles using double-quantum dipolar recoupling solid-state NMR spectroscopy
MA Mehta, MT Eddy, SA McNeill, FD Mills…
Index: Mehta, Manish A.; Eddy, Matthew T.; McNeill, Seth A.; Mills, Frank D.; Long, Joanna R. Journal of the American Chemical Society, 2008 , vol. 130, # 7 p. 2202 - 2212
Several approaches for utilizing dipolar recoupling solid-state NMR (ssNMR) techniques to determine local structure at high resolution in peptides and proteins have been developed. However, many of these techniques measure only one torsion angle or are accurate for only certain classes of secondary structure. Additionally, the efficiency with which these dipolar recoupling experiments suppress the deleterious effects of chemical shift anisotropy (CSA ...