Chemical and Pharmaceutical Bulletin

Fused pyrimidines. IV. The reaction of 4-alkylthio-2-chloroquinazolines with alkylamines in dimethylformamide.

三木秀樹， 山田順二

Index: Miki; Yamada Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 7 p. 2313 - 2318

Full Text: HTML

Citation Number: 2

Abstract

... IR spectra were recorded by using a Hitachi IiPI'3 spectrophotometer, and PMR spectra were taken with a Hitachi R-24 spectrometer; chemical shifts are expressed in ppm (6) from tetramethylsilane as an internal standard. ... H. Miki and J. Yamada, Heterocycles, 19, 10 (1982). ...

 Related Synthetic Route
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

methylamine Structure

74-89-5

methylamine

~92%

2-chloro-N-methyl-quinazolin-4-amine Structure

83260-68-8

2-chloro-N-meth...

2,4-Dichloroquinazoline Structure

607-68-1

2,4-Dichloroqui...

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2-chloro-N-methyl-quinazolin-4-amine Structure

83260-68-8

2-chloro-N-meth...

2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

methylamine Structure

74-89-5

methylamine

~65%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

2-chloro-N-methyl-quinazolin-4-amine Structure

83260-68-8

2-chloro-N-meth...

Detail
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

Dimethylamine Structure

124-40-3

Dimethylamine

~34%

2-dimetylamino-4-methylthioquinazoline Structure

66433-20-3

2-dimetylamino-...

4-dimethylamino-2-methylthioquinazoline Structure

81683-42-3

4-dimethylamino...

Detail
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

Dimethylamine Structure

124-40-3

Dimethylamine

~35%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

2-dimetylamino-4-methylthioquinazoline Structure

66433-20-3

2-dimetylamino-...

Detail
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

~6%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

N/A Structure

69033-44-9

N/A

4-butylamino-2-methylthioquinazoline Structure

81683-40-1

4-butylamino-2-...

Detail
2,4-Dichloroquinazoline Structure

607-68-1

2,4-Dichloroqui...

~%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

methylamine Structure

74-89-5

methylamine

~4%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

2-chloro-N-methyl-quinazolin-4-amine Structure

83260-68-8

2-chloro-N-meth...

Detail
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

Dimethylamine Structure

124-40-3

Dimethylamine

~5%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

2-dimetylamino-4-methylthioquinazoline Structure

66433-20-3

2-dimetylamino-...

Detail
2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...

n-butylamine Structure

109-73-9

n-butylamine

~5%

2,4-bis(methylthio)quinazoline Structure

48141-61-3

2,4-bis(methylt...

N2,N4-dibutylquinazoline-2,4-diamine Structure

81683-41-2

N2,N4-dibutylqu...

Detail
2,4-Dichloroquinazoline Structure

607-68-1

2,4-Dichloroqui...

Sodium thiomethoxide Structure

5188-07-8

Sodium thiomethoxide

~%

2-chloro-4-methylsulfanylquinazoline Structure

66433-07-6

2-chloro-4-meth...


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