1,3-Dichloro-2-iodo-5-nitrobenzene

Modify Date: 2024-01-03 14:02:27

1,3-Dichloro-2-iodo-5-nitrobenzene Structure
1,3-Dichloro-2-iodo-5-nitrobenzene structure
Common Name 1,3-Dichloro-2-iodo-5-nitrobenzene
CAS Number 62778-19-2 Molecular Weight 317.89600
Density 2.158g/cm3 Boiling Point 335.5ºC at 760 mmHg
Molecular Formula C6H2Cl2INO2 Melting Point 153ºC
MSDS N/A Flash Point 156.7ºC

 Names

Name 1,3-Dichloro-2-iodo-5-nitrobenzene
Synonym More Synonyms

 Chemical & Physical Properties

Density 2.158g/cm3
Boiling Point 335.5ºC at 760 mmHg
Melting Point 153ºC
Molecular Formula C6H2Cl2INO2
Molecular Weight 317.89600
Flash Point 156.7ºC
Exact Mass 316.85100
PSA 45.82000
LogP 4.02940
Index of Refraction 1.677

 MSDS


Section I.Chemical Product and Company Identification
Chemical Name 3,5-Dichloro-4-Iodonitrobenzene
Portland OR
1,3-Dichloro-2-iodo-5-nitrobenzene
Synonym
C6H2Cl2INO2
Chemical Formula
CAS Number62778-19-2

Section II.Composition and Information on Ingredients
Chemical NameCAS Number Percent (%)TLV/PELToxicology Data
3,5-Dichloro-4-Iodonitrobenzene62778-19-2Min. Not available.Not available.
99.0%(GC)

Section III. Hazards Identification
Acute Health EffectsNo specific information is available in our data base regarding the toxic effects of this material for humans. However,
exposure to any chemical should be kept to a minimum. Skin and eye contact may result in irritation. May be harmful if
inhaled or ingested. Always follow safe industrial hygiene practices and wear proper protective equipment when handling
this compound.
CARCINOGENIC EFFECTS : Not available.
Chronic Health Effects
MUTAGENIC EFFECTS : Not available.
TERATOGENIC EFFECTS : Not available.
DEVELOPMENTAL TOXICITY: Not available.
Repeated or prolonged exposure to this compound is not known to aggravate existing medical conditions.

Section IV.First Aid Measures
Eye ContactCheck for and remove any contact lenses. In case of contact, immediately flush eyes with plenty of water for at least 15
minutes. Get medical attention.
Skin ContactIn case of contact, immediately flush skin with plenty of water. Remove contaminated clothing and shoes. Wash clothing
before reuse. Thoroughly clean shoes before reuse. Get medical attention.
If the victim is not breathing, perform mouth-to-mouth resuscitation. Loosen tight clothing such as a collar, tie, belt or
Inhalation
waistband. If breathing is difficult, oxygen can be administered. Seek medical attention if respiration problems do not
improve.
IngestionINDUCE VOMITING by sticking finger in throat. Lower the head so that the vomit will not reenter the mouth and throat.
Loosen tight clothing such as a collar, tie, belt or waistband. If the victim is not breathing, perform mouth-to-mouth
resuscitation. Examine the lips and mouth to ascertain whether the tissues are damaged, a possible indication that the
toxic material was ingested; the absence of such signs, however, is not conclusive.

Section V.Fire and Explosion Data
Not available.
Auto-Ignition
FlammabilityMay be combustible at high temperature.
Flash PointsFlammable LimitsNot available.
Not available.
Combustion ProductsThese products are toxic carbon oxides (CO, CO2), nitrogen oxides (NO, NO2), halogenated compounds.
WARNING: Highly toxic HCl gas is produced during combustion.
Fire Hazards
Not available.
Explosion HazardsRisks of explosion of the product in presence of mechanical impact: Not available.
Risks of explosion of the product in presence of static discharge: Not available.
Fire Fighting Media
SMALL FIRE: Use DRY chemical powder.
LARGE FIRE: Use water spray, fog or foam. DO NOT use water jet.
and Instructions
Consult with local fire authorities before attempting large scale fire-fighting operations.
Continued on Next Page
3,5-Dichloro-4-Iodonitrobenzene

Section VI.Accidental Release Measures
Spill CleanupUse a shovel to put the material into a convenient waste disposal container. Finish cleaning the spill by rinsing any
contaminated surfaces with copious amounts of water. Consult federal, state, and/or local authorities for assistance on
Instructions
disposal.

Section VII. Handling and Storage
Keep away from heat. Mechanical exhaust required. When not in use, tightly seal the container and store in a dry, cool
Handling and Storage
place. Avoid excessive heat and light. Do not breathe dust.
Information
Always store away from incompatible compounds such as oxidizing agents.

Section VIII. Exposure Controls/Personal Protection
Engineering ControlsUse process enclosures, local exhaust ventilation, or other engineering controls to keep airborne levels below
recommended exposure limits. If user operations generate dust, fume or mist, use ventilation to keep exposure to
airborne contaminants below the exposure limit.
Personal ProtectionSplash goggles. Lab coat. Dust respirator. Boots. Gloves. Suggested protective clothing might not be sufficient; consult
a specialist BEFORE handling this product. Be sure to use a MSHA/NIOSH approved respirator or equivalent.
Exposure LimitsNot available.

Section IX. Physical and Chemical Properties
Solid. (Light Yellow Crystals.)Solubility
Physical state @ 20°CNot available.
Not available.
Specific Gravity
Molecular Weight317.9Partition CoefficientNot available.
Boiling Point
Not available.Vapor PressureNot applicable.
Melting Point153°C (307.4°F)Vapor DensityNot available.
Refractive IndexNot available.VolatilityNot available.
Critical TemperatureNot available.OdorNot available.
ViscosityNot available.TasteNot available.

Section X.Stability and Reactivity Data
Stability
This material is stable if stored under proper conditions. (See Section VII for instructions)
Conditions of InstabilityAvoid excessive heat and light.
IncompatibilitiesReactive with oxidizing agents.

Section XI. Toxicological Information
Not available.
RTECS Number
Eye Contact. Ingestion. Inhalation.
Routes of Exposure
Toxicity DataNot available.
Chronic Toxic EffectsCARCINOGENIC EFFECTS : Not available.
MUTAGENIC EFFECTS : Not available.
TERATOGENIC EFFECTS : Not available.
DEVELOPMENTAL TOXICITY: Not available.
Repeated or prolonged exposure to this compound is not known to aggravate existing medical conditions.
Acute Toxic EffectsNo specific information is available in our data base regarding the toxic effects of this material for humans. However,
exposure to any chemical should be kept to a minimum. Skin and eye contact may result in irritation. May be harmful if
inhaled or ingested. Always follow safe industrial hygiene practices and wear proper protective equipment when handling
this compound.
Continued on Next Page
3,5-Dichloro-4-Iodonitrobenzene

Section XII.Ecological Information
EcotoxicityNot available.
Not available.
Environmental Fate

Section XIII. Disposal Considerations
Recycle to process, if possible. Consult your local regional authorities. You may be able to dissolve or mix material with a
Waste Disposal
combustible solvent and burn in a chemical incinerator equipped with an afterburner and scrubber system. Observe all
federal, state and local regulations when disposing of the substance.

Section XIV. Transport Information
DOT ClassificationNot a DOT controlled material (United States).
Not applicable.
PIN Number
Proper Shipping Name
Not applicable.
Packing Group (PG)Not applicable.
DOT Pictograms

Section XV. Other Regulatory Information and Pictograms
TSCA Chemical InventoryThis compound is ON the EPA Toxic Substances Control Act (TSCA) inventory list.
(EPA)
WHMIS ClassificationOn NDSL.
(Canada)
EINECS Number (EEC)
Not available.
EEC Risk StatementsNot available.


SECTION 16 - ADDITIONAL INFORMATION
N/A

 Safety Information

HS Code 2904909090

 Synthetic Route

~85%

1,3-Dichloro-2-iodo-5-nitrobenzene Structure

1,3-Dichloro-2-...

CAS#:62778-19-2

Literature: SMITH KLINE and FRENCH LABORATORIES, LIMITED Patent: EP188351 B1, 1991 ;

~33%

1,3-Dichloro-2-iodo-5-nitrobenzene Structure

1,3-Dichloro-2-...

CAS#:62778-19-2

Literature: Anacor Pharmaceuticals, Inc.; Eli Lilly and Company; Akama, Tsutomu; Balko, Terry William; Defauw, Jean Marie; Plattner, Jacob J.; White, William Hunter; Winkle, Joseph Raymond; Zhang, Yong-Kang; Zhou, Yasheen Patent: US2013/131016 A1, 2013 ; Location in patent: Paragraph 0253; 0254 ;

~66%

1,3-Dichloro-2-iodo-5-nitrobenzene Structure

1,3-Dichloro-2-...

CAS#:62778-19-2

Literature: Synthesis, , # 14 p. 2180 - 2190

 Customs

HS Code 2904909090
Summary HS:2904909090 sulphonated, nitrated or nitrosated derivatives of hydrocarbons, whether or not halogenated VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:5.5% General tariff:30.0%

 Synonyms

1,3-dichloro-2-iodo-5-nitro-benzene
1,3-Dichlor-2-jod-5-nitro-benzol
2,6-dichloro-4-nitroiodobenzene
Benzene,1,3-dichloro-2-iodo-5-nitro
3,5-Dichloro-4-iodonitrobenzene